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Laboratories for Thin-Film Synthesis and Characterization

In the thin-film laboratories in Oslo, we synthesize coatings of functional materials for use in, among other things, gas separation membranes, sensors, solar cells, and electrolysis cells.

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Montering av nye prøver, Polyteknik Flextura 800  Foto: SINTEF/Per Martin Rørvik
Installation of new samples, Polyteknik Flextura 800. Photo: SINTEF / Per Martin Rørvik

The lab is dedicated to thin-film processing and is equipped to deposit high-quality thin films with thicknesses ranging from 1 nm to 10 µm on 6'' substrates and on tubes up to 10 cm in length. Metals (Al, Ni, Ti, Pd, etc.), semi-metals (Si, Ge, etc.), metal oxides (TiO₂, SiO₂, YSZ), and nitrides (TiN) are typical material classes processed in the lab. Available deposition techniques include sputtering, electron beam physical vapor deposition (EBPVD), electroplating, and spin coating.

Arbeid inni et av sputterkamrene, Polyteknik Flextura 800 Foto: Lars Andreas Berg
Work inside one of the sputter chambers, Polyteknik Flextura 800. Photo: Lars Andreas Berg

In 2017, we commissioned a unique high-vacuum cluster system (Polyteknik Flextura 800) with two sputtering chambers and one EBPVD chamber. This system enables multilayer deposition without breaking vacuum, co-deposition from up to three targets simultaneously, reactive deposition with N₂ and O₂ in the chamber, and deposition on substrates at high temperatures (up to 1000°C). Samples are loaded through a load-lock chamber and can be transferred between chambers for deposition of different materials. Two of the chambers are equipped with in situ thickness monitors, and substrates can be plasma-etched prior to deposition. The EBPVD chamber is dedicated to silicon deposition (up to 150 µm thick layers). Silicon growth can be studied in situ using RHEED (Reflection High-Energy Electron Diffraction).

Equipment

  • ISO Class 7 cleanroom laboratory
  • Multichamber PVD-based cluster system
  • E-beam (EBPVD) with film thickness up to 150 µm, substrate temperature up to 1000°C (dedicated to silicon)
  • DC, pulsed DC, and RF sputtering on up to 6" Si wafers, substrate temperature up to 800°C (a wide range of materials can be deposited, including reactive deposition with N₂ and O₂)
  • Hydrofluoric acid (HF) fume hood
  • Electroplating
  • Spray coater and spin coater
  • Hot plates up to 400°C
  • Rapid thermal processing (RTP) up to 1200°C
  • Characterization facilities: Electron microscopy (SEM, TEM), white light interferometry (WLI), XRD, XPS, SIMS

Technical Specifications

The laboratories have separate areas for gowning (cleanroom classes 6 and 7) and thin-film processing.

Contact information

Visiting address:
Forskningsveien 1, Oslo